測試對象:巖石、土壤粉末樣品、天然水樣、消解溶液、高純物質雜質等樣品
測試周期:30-45個工作日,全套主微量元素分析可同步進行,周期30-45個工作日??商峁悠窚y試加急服務,加急樣品最短周期20個工作日。
送樣要求:1、樣品量需約2 g,粒度≥200 目,請務必逐個自查,標準為將樣品粉末捻在手心無明顯顆粒感;2、編號清晰,紙袋折疊封裝;3、請勿用訂書機封訂;4、塑料袋包裝或樣品灑出的退回。
完成標準:前處理在超凈室100級超凈臺內進行,保證監測空白及樣品無污染,標樣和重復樣在允許誤差范圍內。
Trace element analysis of whole rock were conducted on Agilent 7700e ICP-MS at the Wuhan SampleSolution Analytical Technology Co., Ltd., Wuhan, China. The detailed sample-digesting procedure was as follows: (1) Sample powder (200 mesh) were placed in an oven at 105 ℃ for drying of 12 hours; (2) 50 mg sample powder was accurately weighed and placed in a Teflon bomb; (3) 1 ml HNO3 and 1 ml HF were slowly added into the Teflon bomb; (4) Teflon bomb was putted in a stainless steel pressure jacket and heated to 190 ℃ in an oven for >24 hours; (5) After cooling, the Teflon bomb was opened and placed on a hotplate at 140 ℃ and evaporated to incipient dryness, and then 1 ml HNO3 was added and evaporated to dryness again; (6) 1 ml of HNO3, 1 ml of MQ water and 1 ml internal standard solution of 1ppm In were added, and the Teflon bomb was resealed and placed in the oven at 190 ℃ for >12 hours; (7) The final solution was transferred to a polyethylene bottle and diluted to 100 g by the addition of 2% HNO3.